

                       INSTRUMENT CONTROL PARAMETERS:    Instrument #1
                       -----------------------------------------------

   C:\MSDCHEM\1\METHODS\RB\FAMES\FAMES-HP5-short.M

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  GC ALS
Mass Spectrometer :  Enabled

=============================================================================
                                6890 GC METHOD
=============================================================================


OVEN
   Initial temp:  50 'C (On)               Maximum temp:  350 'C
   Initial time:  1.00 min                 Equilibration time:  0.25 min
   Ramps:
      #  Rate  Final temp  Final time
      1 50.00      200        0.00
      2  3.00      280        2.00
      3   0.0(Off)
   Post temp:  50 'C
   Post time:  0.00 min
   Run time:  32.67 min


FRONT INLET (SPLIT/SPLITLESS)           BACK INLET (UNKNOWN)
   Mode:  Splitless
   Initial temp:  300 'C (On)
   Pressure:  1.98 psi (On)
   Purge flow:  20.0 mL/min
   Purge time:  0.85 min
   Total flow:  24.4 mL/min
   Gas saver:  Off
   Gas type:  Helium


COLUMN 1                                COLUMN 2
   Capillary Column                        (not installed)
   Model Number:  Agilent 19091J-413
   HP-5  5% Phenyl Methyl Siloxane
   Max temperature:  325 'C
   Nominal length:  30.0 m
   Nominal diameter:  320.00 um
   Nominal film thickness:  0.25 um
   Mode:  constant flow
   Initial flow:  1.5 mL/min
   Nominal init pressure:  1.99 psi
   Average velocity:  45 cm/sec
   Inlet:  Front Inlet
   Outlet:  MSD
   Outlet pressure:  vacuum


FRONT DETECTOR (NO DET)                 BACK DETECTOR (NO DET)


SIGNAL 1                                SIGNAL 2
   Data rate:  20 Hz                       Data rate:  20 Hz
   Type:  test plot                        Type:  test plot
   Save Data:  Off                         Save Data:  Off
   Zero:  0.0 (Off)                        Zero:  0.0 (Off)
   Range:  0                               Range:  0
   Fast Peaks:  Off                        Fast Peaks:  Off
   Attenuation:  0                         Attenuation:  0


COLUMN COMP 1                           COLUMN COMP 2
   (No Detectors Installed)                (No Detectors Installed)


THERMAL AUX 2
   Use:  MSD Transfer Line Heater
   Description:  transfer line
   Initial temp:  300 'C (On)
   Initial time:  0.00 min
      #  Rate  Final temp  Final time
      1   0.0(Off)


                                        POST RUN
                                           Post Time: 0.00 min


TIME TABLE
   Time       Specifier                     Parameter & Setpoint




                               GC Injector


     Front Injector:
        Sample Washes                 0
        Sample Pumps                  0
        Injection Volume           1.00 microliters
        Syringe Size               10.0 microliters
        PreInj Solvent A Washes       3
        PreInj Solvent B Washes       3
        PostInj Solvent A Washes      3
        PostInj Solvent B Washes      3
        Viscosity Delay               0 seconds
        Plunger Speed              Fast
        PreInjection Dwell         0.00 minutes
        PostInjection Dwell        0.00 minutes


     Back Injector:
No parameters specified

 Column 1 Inventory Number : HP5
 Column 2 Inventory Number :  

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : air.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 3.50 min

EM Absolute              : False
EM Offset                : 0
Resulting EM Voltage     : 1764.7

[Scan Parameters]

Low Mass                 : 42.0
High Mass                : 530.0
Threshold                : 100
Sample #                 : 2       A/D Samples    4
Plot 2 low mass          : 42.0
Plot 2 high mass         : 620.0

[MSZones]

MS Quad                  : 150 C   maximum 200 C
MS Source                : 230 C   maximum 250 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: 1
                        -----------------------------

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      23.757
 IONFOCUS    :      82.565
 ENTRANCE_LE :      22.000
 EMVOLTS     :    1764.706
 AMUGAIN     :    1784.000
 AMUOFFSET   :     120.813
 FILAMENT    :       1.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      18.071
 MASSGAIN    :    -652.000   
 MASSOFFSET  :     -39.000   


                           END OF TUNE PARAMETERS
                      ------------------------------------



                            END OF INSTRUMENT CONTROL PARAMETERS
                            ------------------------------------

